A prominent C-acylation-cyclisation synthetic sequence and X-ray structure elucidation of benzothiopyranone derivatives

Kikionis, S; McKee, V; Markopoulos, J; Igglessi-Markopoulou, O

dc.contributor.author	Kikionis, S	en
dc.contributor.author	McKee, V	en
dc.contributor.author	Markopoulos, J	en
dc.contributor.author	Igglessi-Markopoulou, O	en
dc.date.accessioned	2014-03-01T01:27:47Z
dc.date.available	2014-03-01T01:27:47Z
dc.date.issued	2008	en
dc.identifier.issn	0040-4020	en
dc.identifier.uri	https://dspace.lib.ntua.gr/xmlui/handle/123456789/18573
dc.subject	Benzothiopyranones	en
dc.subject	C-Acylation	en
dc.subject	N-Hydroxysuccinimide ester	en
dc.subject	Thiochromones	en
dc.subject	Thiocoumarins	en
dc.subject.classification	Chemistry, Organic	en
dc.subject.other	benzothiopyranone derivative	en
dc.subject.other	ester derivative	en
dc.subject.other	n hydroxysuccinimide	en
dc.subject.other	thiosalicylic acid	en
dc.subject.other	acylation	en
dc.subject.other	article	en
dc.subject.other	chemical structure	en
dc.subject.other	cyclization	en
dc.subject.other	nuclear magnetic resonance	en
dc.subject.other	priority journal	en
dc.subject.other	reaction analysis	en
dc.subject.other	structure analysis	en
dc.subject.other	X ray crystallography	en
dc.title	A prominent C-acylation-cyclisation synthetic sequence and X-ray structure elucidation of benzothiopyranone derivatives	en
heal.type	journalArticle	en
heal.identifier.primary	10.1016/j.tet.2008.04.009	en
heal.identifier.secondary	http://dx.doi.org/10.1016/j.tet.2008.04.009	en
heal.language	English	en
heal.publicationDate	2008	en
heal.abstract	A novel short-step methodology to benzothiopyranone derivatives has been developed starting from an activated precursor, N-hydroxysuccinimide ester of thiosalicylic acid. The procedure is based on a tandem C-acylation-cyclisation process under mild reaction conditions in good yields. The structure elucidation has been established using X-ray crystallography and NMR spectral data. (C) 2008 Elsevier Ltd. All rights reserved.	en
heal.publisher	PERGAMON-ELSEVIER SCIENCE LTD	en
heal.journalName	Tetrahedron	en
dc.identifier.doi	10.1016/j.tet.2008.04.009	en
dc.identifier.isi	ISI:000256412800004	en
dc.identifier.volume	64	en
dc.identifier.issue	23	en
dc.identifier.spage	5454	en
dc.identifier.epage	5458	en