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Development of a precursor sol for the electric field assisted sol-gel deposition of yttrium silicate

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dc.contributor.author Grosse-Brauckmann, J en
dc.contributor.author Lezniak, A en
dc.contributor.author Argirusis, C en
dc.contributor.author Borchardt, G en
dc.date.accessioned 2014-03-01T01:33:09Z
dc.date.available 2014-03-01T01:33:09Z
dc.date.issued 2010 en
dc.identifier.issn 0927-7757 en
dc.identifier.uri https://dspace.lib.ntua.gr/xmlui/handle/123456789/20346
dc.subject Electrophoretic deposition en
dc.subject Oxidation resistance en
dc.subject Sol-gel en
dc.subject Yttrium silicate en
dc.subject.classification Chemistry, Physical en
dc.subject.other Aging time en
dc.subject.other Assisted deposition en
dc.subject.other Carbon composites en
dc.subject.other Carbon fibres en
dc.subject.other Concentrated sols en
dc.subject.other Deposition process en
dc.subject.other Dynamic light scattering method en
dc.subject.other Effect of water en
dc.subject.other Electrophoretic deposition en
dc.subject.other Electrophoretic depositions en
dc.subject.other Growth mechanisms en
dc.subject.other Hydrolysis and condensation en
dc.subject.other Iso-propoxide en
dc.subject.other Outer layer en
dc.subject.other Particle charge en
dc.subject.other Sol particles en
dc.subject.other Sol-gel deposition en
dc.subject.other Synthesis parameters en
dc.subject.other Synthesis route en
dc.subject.other Tetraethoxysilanes en
dc.subject.other Yttrium silicates en
dc.subject.other Carbon carbon composites en
dc.subject.other Carbon fibers en
dc.subject.other Electric fields en
dc.subject.other Electrophoresis en
dc.subject.other Gels en
dc.subject.other Glassy carbon en
dc.subject.other Light scattering en
dc.subject.other Oxidation en
dc.subject.other Oxidation resistance en
dc.subject.other pH effects en
dc.subject.other Silicates en
dc.subject.other Silicon carbide en
dc.subject.other Sol-gel process en
dc.subject.other Sol-gels en
dc.subject.other Sols en
dc.subject.other Yttrium en
dc.subject.other Yttrium alloys en
dc.subject.other carbon en
dc.subject.other carbon fiber en
dc.subject.other monomer en
dc.subject.other nanocomposite en
dc.subject.other silicon en
dc.subject.other yttrium en
dc.subject.other yttrium silicate y 90 en
dc.subject.other article en
dc.subject.other electric field en
dc.subject.other gelation en
dc.subject.other hydrodynamics en
dc.subject.other hydrolysis en
dc.subject.other light scattering en
dc.subject.other melting point en
dc.subject.other microelectrophoresis en
dc.subject.other particle radiation en
dc.subject.other pH en
dc.subject.other polymerization en
dc.subject.other priority journal en
dc.subject.other viscosity en
dc.subject.other X ray diffraction en
dc.subject.other zeta potential en
dc.title Development of a precursor sol for the electric field assisted sol-gel deposition of yttrium silicate en
heal.type journalArticle en
heal.identifier.primary 10.1016/j.colsurfa.2010.01.014 en
heal.identifier.secondary http://dx.doi.org/10.1016/j.colsurfa.2010.01.014 en
heal.language English en
heal.publicationDate 2010 en
heal.abstract In this paper we present a synthesis route for an Y2SiO5 sol derived from tetraethoxysilane and yttrium oxo-isopropoxide where the sot particles show a significant particle charge. The dynamic light scattering method was applied to obtain information on the relation between charging and growth of these sol species. The effect of water concentration, pH of the employed water and aging time on hydrolysis and condensation on the amount of charging and the growth mechanism of sol particles were investigated. Synthesis parameters were optimized to allow an electric field assisted deposition of the sot-get particles from low concentrated sols. Glassy carbon and carbon fibre reinforced carbon composites with a silicon/silicon carbide outer layer (C/C-SiC) were used as substrates for the deposition process. (C) 2010 Elsevier BM. All rights reserved. en
heal.publisher ELSEVIER SCIENCE BV en
heal.journalName Colloids and Surfaces A: Physicochemical and Engineering Aspects en
dc.identifier.doi 10.1016/j.colsurfa.2010.01.014 en
dc.identifier.isi ISI:000276115100005 en
dc.identifier.volume 358 en
dc.identifier.issue 1-3 en
dc.identifier.spage 28 en
dc.identifier.epage 34 en


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