Doping control analysis in human urine by liquid chromatography–electrospray ionization ion trap mass spectrometry for the Olympic Games Athens 2004: Determination of corticosteroids and quantification of ephedrines, salbutamol and morphine

Spyridaki, M; Kiousi, P; Vonaparti, A; Valavani, P; Zonaras, V; Zahariou, M; Sianos, E; Tsoupras, G; Georgakopoulos, C

dc.contributor.author	Spyridaki, M	en
dc.contributor.author	Kiousi, P	en
dc.contributor.author	Vonaparti, A	en
dc.contributor.author	Valavani, P	en
dc.contributor.author	Zonaras, V	en
dc.contributor.author	Zahariou, M	en
dc.contributor.author	Sianos, E	en
dc.contributor.author	Tsoupras, G	en
dc.contributor.author	Georgakopoulos, C	en
dc.date.accessioned	2014-03-01T01:54:55Z
dc.date.available	2014-03-01T01:54:55Z
dc.date.issued	2006	en
dc.identifier.uri	https://dspace.lib.ntua.gr/xmlui/handle/123456789/27531
dc.subject	electrospray ionization	en
dc.subject	electrospray ionization mass spectrometry	en
dc.subject	Ion Trap	en
dc.subject	Limit of Detection	en
dc.subject	Liquid Chromatography	en
dc.subject	Mass Spectrometry	en
dc.subject	Olympic Games	en
dc.subject	Limit of Quantification	en
dc.title	Doping control analysis in human urine by liquid chromatography–electrospray ionization ion trap mass spectrometry for the Olympic Games Athens 2004: Determination of corticosteroids and quantification of ephedrines, salbutamol and morphine	en
heal.type	journalArticle	en
heal.identifier.primary	10.1016/j.aca.2006.04.042	en
heal.identifier.secondary	http://dx.doi.org/10.1016/j.aca.2006.04.042	en
heal.publicationDate	2006	en
heal.abstract	A new liquid chromatography–electrospray ionization-mass spectrometry (LC–ESI–MS) (n) ion trap method for the determination of corticosteroids in urine has been developed and validated. Some anabolic agents, such as epitrenbolone, trenbolone, 2-hydroxymethylformebolone, tetrahydrogestrinone, gestrinone and formoterol were included in the LC–ESI–MS method. Matrix interference, specificity, identification capability, carry over and robustness were estimated as validation parameters. Recoveries ranged from 74 to	en
heal.journalName	Analytica Chimica Acta	en
dc.identifier.doi	10.1016/j.aca.2006.04.042	en