dc.contributor.advisor |
Κορδάτος, Κωνσταντίνος |
el |
dc.contributor.author |
Μιχαήλ, Άγγελος Κ.
|
el |
dc.contributor.author |
Michael, Aggelos K.
|
en |
dc.date.accessioned |
2014-10-31T10:51:43Z |
|
dc.date.available |
2014-10-31T10:51:43Z |
|
dc.date.copyright |
2014-05-28 |
- |
dc.date.issued |
2014-10-31 |
|
dc.date.submitted |
2014-05-28 |
- |
dc.identifier.uri |
https://dspace.lib.ntua.gr/xmlui/handle/123456789/39446 |
|
dc.identifier.uri |
http://dx.doi.org/10.26240/heal.ntua.5694 |
|
dc.description |
60 σ. |
el |
dc.description.abstract |
|
el |
dc.description.abstract |
The aim of this thesis was the synthesis and characterization of fullerene
derivatives.More specifically has been the synthesis and characterization of two
derivatives of fullerenes : C82H21N5O10 and C82H24N2O4 .Firstly held the preparation of
a-amino acid which was used in subsequent cycloaddition reaction with the
fullerene.Then after decarboxylation of alpha-amino acid is reacted with an aldehyde
and fullerene in an organic solvent under heating (Prato’s reaction), resulting the
synthesis of fouleropyrolidinis.Then took place the synthesis of 2-5-7-
trinitrofluorenone-4-carboxylic acid, where this product is reacted with
fouleropyrolidini and formed the derivative, C82H21N5O10. For the formation of the
second derivative , C82H24N2O4, reaction took place between fouleropyrolidinis and
flouorenonis-4-carboxylic acid. Then these two derivatives of fullerene characteristic
withmass spectrometry and FT-IR spectomertry. |
en |
dc.description.statementofresponsibility |
Άγγελος Κ. Μιχαήλ |
el |
dc.language.iso |
el |
en |
dc.rights |
ETDFree-policy.xml |
en |
dc.subject |
Φουλερένιο |
el |
dc.subject |
Σύνθεση |
el |
dc.subject |
Φουλεροπυρολιδίνη |
el |
dc.subject |
Τρινιτροφλουορενόνη |
el |
dc.subject |
Χαρακτηρισμός |
el |
dc.subject |
Fullerene |
en |
dc.subject |
Synthesis |
en |
dc.subject |
Fouleropyrolidinis |
en |
dc.subject |
Trinifluorenone |
en |
dc.subject |
Characterization |
en |
dc.title |
Σύνθεση και χαρακτηρισμός παραγώγων του φουλερένιου |
el |
dc.title.alternative |
Synthesis and characterization of fullerence derivatives |
en |
dc.type |
bachelorThesis |
el (en) |
dc.date.accepted |
2014-04-14 |
- |
dc.date.modified |
2014-05-28 |
- |
dc.contributor.advisorcommitteemember |
Χαμηλάκης, Στυλιανός |
el |
dc.contributor.advisorcommitteemember |
Λιοδάκης, Στυλιανός |
el |
dc.contributor.committeemember |
Κορδάτος, Κωνσταντίνος |
el |
dc.contributor.committeemember |
Χαμηλάκης, Στυλιανός |
el |
dc.contributor.committeemember |
Λιοδάκης, Στυλιανός |
el |
dc.contributor.department |
Εθνικό Μετσόβιο Πολυτεχνείο. Σχολή Χημικών Μηχανικών. Τομέας Χημικών Επιστημών. Εργαστήριο Ανόργανης και Αναλυτικής Χημείας. |
el |
dc.date.recordmanipulation.recordcreated |
2014-10-31 |
- |
dc.date.recordmanipulation.recordmodified |
2014-10-31 |
- |